MAPEX Instrument Database
X-Ray Powder
General information
Description
X-ray powder diffractometer Stadi MP
Manufacturer
Stoe & Cie GmbH, Darmstadt
Category
Diffraction, Structure characterization, non-ambient X-ray powder diffraction, in-situ reaction studies
MAPEX Category
Surface / Interface Characterization, Material Properties
Keywords
Powder diffraction, temperate-dependent structure characterization, X-ray powder diffraction
Measured Quantity
X-ray diffraction patterns
Main Application
structure determination and refinement from temperature-dependent X-ray data
Year of Fabrication
12/2017
Instrument specification
Specifications
- Ge(111) monochromized Mo radiation
- Transmission (capillary and flat samples) and reflection geometry
- Dectris Mythen 1k linear detector (18° 2θ width) allowing for energy discrimination to suppress sample fluorescence and fast data collection for e.g. observation of reaction kinetics
- Stoe insituHT2 heating chamber allows for application of different gases while heating (300 K – 1873 K)
- Oxford Cryosystems PheniX He-closedcycle cooling chamber (12 K – 310 K)
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Contact
Contact person
Lars Robben
Fachbereich 2 / IACK
NW2/C3051
Phone +49 421 218 63142
lrobben@uni-bremen.de
Principal Investigator
Gesing, Thorsten