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MAPEX Instrument Database

X-Ray Powder

General information

Description
X-Ray Powder Defractometer Stadimp
Manufacturer
Stoe & Cie GmbH, Darmstadt
Category
Diffraction, Structure characterization, non-ambient X-ray powder diffraction, in-situ reaction studies
MAPEX Category
Surface / Interface Characterization, Material Properties
Keywords
Powder diffraction, temperate-dependent structure characterization, X-ray powder diffraction
Measured Quantity
diffraction patterns
Main Application
structure determination and refinement from temperature-dependent X-ray data
Year of Fabrication
12/2017

Instrument specification

Specifications
  • Ge(111) monochromized Mo radiation
  •  Transmission (capillary and flat samples) and reflection geometr
  • Dectris Mythen 1k linear detector (18° 2θ width) allowing for energy discrimination to suppress sample fluorescence and fast data collection for e.g. observation of reaction kinetics
  • Stoe insituHT2 heating chamber allows for application of different gases while heating (300 K – 1873 K)
  • Oxford Cryosystems PheniX He-closedcycle cooling chamber (12 K – 310 K)

 

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Contact

Contact person

Lars Robben
Fachbereich 2 / IACK
NW2/C3051
Phone +49 421 218 63142
lrobben@uni-bremen.de

Principal Investigator
Gesing, Thorsten
Updated by: MAPEX