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X-Ray Diffraction Highlights

Quantitative three-dimensional local order analysis
© 2023 The Authors
MAPEX Research Highlights|

Quantitative three-dimensional local order analysis of nanomaterials through electron diffraction

Ella Mara Schmidt; Paul Benjamin Klar; Yasar Krysiak; Petr Svora; Andrew L. Goodwin; Luke Palatinus

Nature Communications, 14 (2023)

doi:  10.1038/s41467-023-41934-y

Structure-property relationships in ordered materials have long been a core principle in materials design. However, the…

Figure from the publication
© 2022 Walter de Gruyter GmbH, Berlin/Boston
Materials Modelling| X-Ray Diffraction|

Halide-sodalites: thermal behavior at low temperatures and local deviations from the average structure

Marius Wolpmann, Martin Etter, Andrea Kirsch, Filippo Balzaretti, Wilke Dononelli, Lars Robben and Thorsten M. Gesing

Zeitschrift für Kristallographie - Crystalline Materials238 (2023), 27 - 38

https://doi.org/10.1515/zkri-2022-0037

Sodalites of the general type |Na8X2|[T1T2O4]6 with X = Cl−, Br…

SEM image
© © 2022 The Authors. Zeitschrift für anorganische und allgemeine Chemie published by Wiley-VCH GmbH
Correlated Workflows| In-situ, real-time investigations| X-Ray Diffraction| Spectroscopy| Electron Microscopy|

On red tin (II) oxide: temperature-dependent structural, spectroscopic, and thermogravimetric properties

Sarah Wittmann,  M. Mangir Murshed,  Thorsten M. Gesing

Z. Anorg. Allg. Chem. 2022, 648, e20220031

https://doi.org/10.1002/zaac.202200311

Polycrystalline red tin(II)oxide (RSO) has been synthesized by a fast reflux method. X-ray powder diffraction (XRPD) data Rietveld refinement confirms the…

picture
© The Royal Society of Chemistry 2022
Correlated Workflows| In-situ, real-time investigations| X-Ray Diffraction|

Effects of iron substitution and anti-site disorder on crystal structures, vibrational, optical and magnetic properties of double perovskites Sr2(Fe1−xNix)TeO6

Asmaa Zaraq, Duncan H. Gregory, Brahim Orayech, Josu M. Igartua,Abdeslam El Bouari,James D. Eales, Paul A. Binghamand Thorsten M. Gesing

Dalton Transactions (2022)

https://doi.org/10.1039/D2DT02447K

The double-perovskite series, Sr2(Fe1−xNix)TeO6 (x = 0, 0.25, 0.50, 0.75, and 1) has been…

picture
© https://doi.org/10.1007/s10853-022-07854-w, CC BY 4.0
X-Ray Diffraction| Spectroscopy|

Nano-crystalline precursor formation, stability, and transformation to mullite-type visible-light photocatalysts

Thorsten M. Gesing, M. Mangir Murshed, Selina Schuh, Oliver Thüringer, Konrad Krämer, Tim Neudecker, Cecilia B. Mendive & Lars Robben 

Journal of Materials Science (2022), 57, 19280-19299

https://doi.org/10.1007/s10853-022-07854-w

A new precursor for the formation of mullite-type visible-light…

Picture
© Reprinted with permission from https://doi.org/10.1021/acs.cgd.2c00030. Copyright 2022 American Chemical Society.
X-Ray Diffraction|

Revisiting the Growth of Large (Mg,Zr):SrGa12O19 Single Crystals: Core Formation and Its Impact on Structural Homogeneity Revealed by Correlative X-ray Imaging

Christo Guguschev, Carsten Richter, Mario Brützam, Kaspars Dadzis, Christian Hirschle, Thorsten M. Gesing, Michael Schulze, Albert Kwasniewski, Jürgen Schreuer, and Darrell G. Schlom

Crystal Growth and Design (2022), 22, 4, 2557–2568

https://doi.org/10.1021/acs.cgd.2c00030

We demonstrate the…

X-Ray Diffraction|

Halide-sodalites: thermal expansion, decomposition and the Lindemann criterion

Marius Wolpmann, Lars Robben and Thorsten M. Gesing

Zeitschrift für Kristallographie - Crystalline Materials (2022), 237, 1-3

https://doi.org/10.1515/zkri-2022-0004

Twelve cubic sodalites |Na8X2|[T1T2O4]6 (T1 = Al3+, Ga3+; T2 = Si4+, Ge4+; X = Cl−, Br−, I−) were examined using high-temperature…

X-Ray Diffraction|

Crystal structure and temperature-dependent properties of Na2H4Ga2GeO8 – a novel gallogermanate

Irma Peschke, Lars Robben, Christof Köhler, Thomas Frauenheim, Josef-Christian Buhl and Thorsten M. Gesing

Zeitschrift für Naturforschung B (2020), 75, 9-10

https://doi.org/10.1515/znb-2020-0159

Synthesis, crystal structure and temperature-dependent behavior of Na2H4Ga2GeO8 are reported. This…

X-Ray Diffraction|

On the nature of the phase transitions of aluminosilicate perrhenate sodalite

Kowsik Ghosh, M. Mangir Murshed, Thomas Frederichs, Naveen K. C. Muniraju, Thorsten M. Gesing

Zeitschrift für Kristallographie - Crystalline Materials (2020), 235, 6-7

https://doi.org/10.1515/zkri-2020-0027

The temperature-dependent structure-property relationships of the aluminosilicate…

X-Ray Diffraction|

Low-temperature anharmonicity and symmetry breaking in the sodalite |Na8I2|[AlSiO4]6

Lars Robben, Isaac Abrahams, Michael Fischer, Stephen Hull, Martin T. Dove und Thorsten M. Gesing

Zeitschrift für Kristallographie - Crystalline Materials (2018) 234, Heft 4

https://doi.org/10.1515/zkri-2018-2122

The aluminosilicate iodide sodalite |Na8I2|[AlSiO4]6 was examined by…

X-Ray Diffraction|

Temperature-dependent Structural and Spectroscopic Studies of (Bi1–xFex)FeO3

Andrea Kirsch, M. Mangir Murshed, Melanie J. Kirkham, Ashfia Huq, F. Jochen Litterst and Thorsten M. Gesing

The Journal of Physical Chemistry C (2018) 122 (49), 28280–28291

https://doi.org/10.1021/acs.jpcc.8b05740

We report on temperature-dependent structural and spectroscopic features of (Bi1–xF…

X-Ray Diffraction|

Structural and spectroscopic comparison between polycrystalline, nanocrystalline and quantum dot visible light photo-catalyst Bi2WO6

Michael Teck, M. Mangir Murshed, Marco Schowalter, Niels Lefeld, Henrike K. Grossmann, Tim Grieb, Thomas Hartmann, Lars Robben, Andreas Rosenauer, Lutz Mädler, Thorsten M.Gesing

Journal of Solid State Chemistry (2017) 254, 82-89 

https://doi.org/10.1016/j.jssc.2017.07.013

The structural and…

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